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Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 2023 France English Publisher:Royal Society of Chemistry (RSC)Journal:Chemical Science, volume 14, pages 10,121-10,128 (issn: 2041-6520, eissn: 2041-6539, Copyright policy )Funded by:EC | STRUCTURE
Authors: Samuel F. Cousin; Colan E. Hughes; Fabio Ziarelli; Stéphane Viel; Giulia Mollica; Kenneth D. M. Harris; Arthur C. Pinon; +1 Authors

doi: 10.1039/d3sc02063k , 10.5281/zenodo.8019697 , 10.5281/zenodo.8019696

pmid: 37772100

pmc: PMC10530703

Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material

Abstract

Solid-state DNP NMR is applied to detect a small amount of a minor polymorph of an organic material within a major polymorphic phase, yielding quantitative details of the spatial distribution of the two polymorphs within particles in a powder sample.

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Keywords

Chemistry, Sensitivity, Hyperpolarization, Dynamic nuclear polarization, morphology, [CHIM] Chemical Sciences, DNP, Polymorphism, spin diffusion, NMR, Spectroscopy, Nuclear magnetic resonance

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selected citations
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This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
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