Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2

descriptionPublicationkeyboard_double_arrow_right Article 17 Aug 2018 Spain, France English Publisher:MathDoc/Centre MersenneJournal:Comptes Rendus. Chimie, volume 21, pages 809-813 (issn: 1631-0748, eissn: 1878-1543,

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Authors: Cormary, Benoit; Faulmann, C.; Caro, Dominique; Valade, Lydie; Caro, P.; Ballesteros, B.; Fraxedas, J.;

doi: 10.1016/j.crci.2018.07.006

handle: 10261/199194

Facile synthesis of nanoparticles of the molecule-based superconductor κ-(BEDT-TTF)2Cu(NCS)2

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Abstract

Well-dispersed roughly spherical nano-objects of the molecule-based superconductor κ-(BEDT-TTF) 2 Cu(NCS) 2 have been prepared in an organic solution by using an easy synthetic route. Long alkyl-chain aconitate esters have been used as growth controlling agents. Nano-objects exhibiting sizes in the 35–120 nm range are made of aggregated individual smaller nanoparticles ranging from 3 to 10 nm. Nanoparticle powders have been studied by X-ray diffraction, high resolution electron microscopy and atomic force microscopy in the conductivity mode.

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Keywords

[SPI.GPROC] Engineering Sciences [physics]/Chemical and Process Engineering, Matériaux, Donor–acceptor systems, [SPI.MAT] Engineering Sciences [physics]/Materials, 530, [SPI.MAT]Engineering Sciences [physics]/Materials, 620, Nanostructures, Systèmes donneur–accepteur, Electron microscopy, [SPI.GPROC]Engineering Sciences [physics]/Chemical and Process Engineering, Microscopie électronique, Supraconducteurs, Superconductors, Génie des procédés, Donor-acceptor systems

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