Cis- and trans-fused Di-tetrahydropyrans by rearrangement of steroidal spiroacetals

descriptionPublicationkeyboard_double_arrow_right Article 01 Oct 1995 English Publisher:Elsevier BVJournal:Tetrahedron Letters, volume 36, pages 7,309-7,312 (issn: 0040-4039,

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Authors: Dorta, Rosa L.; Freire, Raimundo; Martín, Ángeles; Suárez, Ernesto; Prangé, Thierry;

doi: 10.1016/0040-4039(95)01472-t

handle: 10261/17230

Cis- and trans-fused Di-tetrahydropyrans by rearrangement of steroidal spiroacetals

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Abstract

This work was supported by the Investigation Programme n ° PB93-0171 of the Dirección General de Investigación Científica y Técnica. A. M. thanks the Ministerio de Educación y Ciencia, Spain, for a fellowship.

A new method for the synthesis of steroidal cis- and trans-fused di-tetrahydropyrans (1,6-dioxadecalins) by reduction with DIBAH of derivatives of 1,6-dioxaspiro[4,5]decan-10-yl methanesulfonate is described.

4 pages, 2 figures, 3 schemes.

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