3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

descriptionPublicationkeyboard_double_arrow_right Article 16 Oct 2012 Cyprus English Publisher:MDPI AGJournal:Molbank, volume 2,012, page M782 (eissn: 1422-8599,

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Authors: Ioannidou, Heraklidia A.; Koutentis, Panayiotis Andreas; Ioannidou, Heraklidia A.; Koutentis, Panayiotis Andreas;

doi: 10.3390/m782

3-Chloro-5-(4-dodecylthiophen-2-yl)-4H-1,2,6-thiadiazin-4-one

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Abstract

3-Chloro-5-trifluoromethanesulfonate-4H-1,2,6-thiadiazin-4-one 3 reacts with (4-dodecylthiophen-2-yl)trimethylstannane 5 (1 equiv.) in the presence of Pd(Ph3P)2Cl2 (5 mol%) in benzene at ca. 20 °C for 5 h to give 3-chloro-5-(4-dodecylthien-2-yl)-1,2,6-thiadiazinone 6 in 87% yield.

Country

Cyprus

Related Organizations

University of Cyprus
Cyprus

Keywords

heterocycles, thiophenes, Oligomers, 1,2,6-thiadiazines, Heterocycles, Thiophenes, oligomers, Inorganic chemistry, QD146-197

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