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Acta Stomatologica Croatica
Article . 2016 . Peer-reviewed
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Acta Stomatologica Croatica
Article
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Acta Stomatologica Croatica
Article . 2016
Data sources: DOAJ
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Long Term Degree of Conversion of two Bulk-Fill Composites

Dugoročna naknadna polimerizacija dvaju „bulk-fill” kompozita
Authors: Par, Matej; Lapaš Barišić, Matea; Gamulin, Ozren; Pandurić, Vlatko; Španović, Nika; Tarle, Zrinka;

Long Term Degree of Conversion of two Bulk-Fill Composites

Abstract

To investigate the long-term development of the post-cure degree of conversion (DC) for two flowable bulk-fill composites.Tetric EvoFlow Bulk Fill (TEFBF) and SDR were chosen due to their distinct compositional modifications that enable the decrease of translucency during polymerization and lower polymerization rate, respectively. DC was assessed using FT-Raman spectroscopy at the post-cure times of 0 h, 24 h, 7 d and 30 d. The post-cure behavior was analyzed by a mixed model ANOVA and partial eta-squared statistics.DC ranged from 61.3-81.1% for TEFBF and 58.9-81.6% for SDR. The initial (0 h) DC was significantly lower at a depth of 4 mm than at a depth of 1 mm (4.9% for SDR and 11.1% for TEFBF). Both materials presented a significant post-cure DC increase, up to 16.4% for TEFBF and 20.6% for SDR. The post-cure DC development was depth-dependent for TEFBF, but not for SDR. The post-cure DC increase was observed during 24 h for TEFBF and 7 d for SDR.Some of the bulk-fill composites may need longer times than the commonly accepted 24 h to reach the final conversion. This may be attributed to their compositional modifications that are mostly undisclosed by manufacturers. Our findings imply that investigations commonly performed 24 h post-cure may underestimate some of the bulk-fill composite properties, if these are affected by the slowly-developing DC. Reactive species may also be available for leaching out of the restoration during an extended time period, with possible implications on biocompatibility.

Country
Croatia
Keywords

Bulk-fill composite ; Photopolymerization ; Post-cure polymerization ; Degree of conversion ; Raman spectroscopy, Photopolymerization, Degree of conversion, Bulk-fill composite, RK1-715, Spectrum Analysis, Raman, Composite Resins, Polymerization, Kliničke medicinske znanosti, Post-cure polymerization, Biomedicina i zdravstvo, Dentistry, Clinical Medical Sciences, Raman spectroscopy, Biomedicine and Health Sciences

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    popularity
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    influence
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    impulse
    This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
    Top 10%
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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
31
Top 10%
Top 10%
Top 10%
Green
Published in a Diamond OA journal