Maximum likelihood estimates of the free parameters, and an asymptotic likelihood-ratio test, are given for the hypothesis that one or more elements of a covariance matrix are zero, and/or that two or more of its elements are equal. The theory applies immediately to a transformation of the covariance matrix by a known nonsingular matrix. Estimation is by Newton's method, starting conveniently from a closed-form least-squares solution.Numerical illustrations include a test for equality of diagonal blocks of a covariance matrix, and estimation of quasi-simplex structures.