AbstractOn the Matmata Plateau, the sedimentological characteristics of the peri‐desert loess and the interbedded palaeosols (particle‐size distribution; chemical and mineralogical composition of major components; trace elements; clay mineral assemblage; heavy mineral assemblage; SEM‐examined surficial textures of the quartz and palygorskite grains) show notable homogeneity: they also indicate its allochthonous origins (the main sedimentary source being the Great Eastern Erg), its transport as an aeolian suspension sediment prior to deposition, and moderate pedogenesis acting during deposition.The emplacement of the loess was synchronous with a ‘pluvial’ steppe palaeoenvironment moister than at present, as shown by 18O and 13C data. The palaeosols point to a weak pedogenesis and colluvial and alluvial reworking that were contemporary with the aeolian deposition. 14C radiometric dating suggests a main period of pluvial dust‐fall/loess deposition in the Upper Pleistocene (until 10 000 yr BP) and a shorter one in the Middle Holocene.