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REFINING POROSITY ANALYSIS IN HIGH-STRENGTH MICROCONCRETES THROUGH MANUAL THRESHOLD SEGMENTATION IN X-RAY MICROTOMOGRAPHY

Authors: Silva, Arthur Aviz Palma E; Valdirene Maria Silva Capuzzo; Eugênia Fonseca Da Silva; Pereira, André Maués Brabo;

REFINING POROSITY ANALYSIS IN HIGH-STRENGTH MICROCONCRETES THROUGH MANUAL THRESHOLD SEGMENTATION IN X-RAY MICROTOMOGRAPHY

Abstract

{"references": ["Pereira, A. (2016). Experi\u00eancias na engenharia da UFF com micro tomografia de raios-X. Hist\u00f3ria, hist\u00f3rias, 2(11), 18-33.", "Landis, E. N., Nagy, E. N., & Keane, D. T. (1997). Microtomographic measurements of internal damage in portland-cement-based composites. Journal of Aerospace Engineering, 10(1), 2-6.", "Bernardes, E. E., de Magalh\u00e3es, A. G., Vasconcelos, W. L., Carrasco, E. V. M., Nunes, E. H. H., & de Lima, L. B. (2017). Characterization of test specimens produced in reduced size for X-ray microtomography (\u00b5-CT) tests. Revista IBRACON de Estruturas e Materiais, 10(5), 1025-1041. http://dx.doi.org/10.1590/s1983-41952017000500005", "Vianna, R. S., Silva, L. C., Lopes, R. T., Ribeiro, L. M., & De Andrade, R. J. (2020). Computing Effective Permeability of Porous Media with FEM and Micro-CT: An Educational Approach. Fluids, 5(1), 16. (4)", "Rattanasak, U., & Kendall, K. (2005). Pore structure of cement/pozzolan composites by X-ray microtomography. Cement and Concrete Research, 35, 637-640.", "Palma e Silva, A. A., Capuzzo, V. M. S., Silva, E. F., Pereira, A. M. B., & e Silva, D. A. P. (2022). Evaluation of mechanical properties and microstructure of high-performance mortars with superabsorbent polymers and metakaolin by means of X-ray computed microtomography. Journal of Building Engineering, 51, 104219.", "Meira, S. A., Sacramento, L. A., Lima, M. P., de Castro Pess\u00f4a, J. R., de Almeida Nascimento, F. L., & de Assis, J. T. (2020). An\u00e1lise da porosidade de concreto por processamento de imagem: uma vis\u00e3o da sensibilidade do Threshold na binariza\u00e7\u00e3o. Brazilian Journal of Development, 6(3), 16449-16459", "Enr\u00edquez-Le\u00f3n, A. J., de Souza, T. D., Arag\u00e3o, F. T. S., Braz, D., Pereira, A. M. B., & Nogueira, L. P. (2021). Determination of the air void content of asphalt concrete mixtures using artificial intelligence techniques to segment micro-CT images. International Journal of Pavement Engineering, 1-10.", "ASSOCIA\u00c7\u00c3O BRASILEIRA DE NORMAS T\u00c9CNICAS. (2018). NBR, ABNT 16697: Cimento Portland \u2014 Requisitos. Rio de Janeiro.", "ASSOCIA\u00c7\u00c3O BRASILEIRA DE NORMAS T\u00c9CNICAS. (2018). NBR, ABNT. 16607: Cimento Portland\u2014Determina\u00e7\u00e3o dos tempos de pega. Rio de Janeiro: ABNT.", "ASSOCIA\u00c7\u00c3O BRASILEIRA DE NORMAS T\u00c9CNICAS. (2017). NBR, ABNT. 16605: Cimento Portland e outros materiais em p\u00f3: determina\u00e7\u00e3o da massa espec\u00edfica", "ASSOCIA\u00c7\u00c3O BRASILEIRA DE NORMAS T\u00c9CNICAS. (2019). NBR NM 67:2019 - Concreto - Determina\u00e7\u00e3o da resist\u00eancia \u00e0 compress\u00e3o de corpos de prova cil\u00edndricos. Rio de Janeiro: ABNT.", "ASSOCIA\u00c7\u00c3O BRASILEIRA DE NORMAS T\u00c9CNICAS. (2010). NBR 7211:2010 - Agregados para concreto - Especifica\u00e7\u00e3o. Rio de Janeiro: ABNT", "RILEM. (2012). State-of-the-art report of the Rilem Technical Committee 225-SAP: Application of superabsorbent polymers (SAP) in concrete construction. Mechtcherine, V. & Reinhardt, H.W. (Eds.). London: Ed. Springer. (12)", "Deutsches Institut f\u00fcr Normung. (1982). 18555-2: Testing of mortars containing mineral binders, freshly mixed mortars containing aggregates of dense structure (heavy aggregates), determination of consistence, bulk density and air content. DIN, Germany", "Gomes, O. F. M. (2001). Processamento e An\u00e1lise de Imagens Aplicados \u00e0 Caracteriza\u00e7\u00e3o Autom\u00e1tica de Materiais. Disserta\u00e7\u00e3o apresentada ao Departamento de Ci\u00eancia de Materiais e Metalurgia da PUC/Rio como parte dos requisitos para a obten\u00e7\u00e3o do t\u00edtulo de Mestre em Ci\u00eancias da Engenharia Metal\u00fargica", "Aboufoul, M., & Garcia, A. (2017). Factors affecting hydraulic conductivity of asphalt mixture. Materials and Structures, 50(1), 1-16.", "Schindelin, J. (2012). FIJI. An Open-Source Platform for Biological-Image Analysis. Nature Methods, 9, 676-68. (17)", "Mattana, A. J., Pereira, E., & Costa, M. M. M. (2014). Evaluation Of Porosity In Mortar By X-Ray Microtomography (Micro-CT). As an additional tool for mercury intrusion porosimetry. Iberoamerican Journal of Applied Computing, 4(1).", "Promentilla, M. A. B., & Sugiyama, T. (2010). X-Ray Microtomography of Mortars Exposed to Freezing-Thawing Action. Journal of Advanced Concrete Technology, 8(2), 97-111.", "Augusto, K. S., & Paciornik, S. (2017). Porosity characterization of iron ore pellets by X-ray microtomography. Materials Research, 21(2), e2017062.", "Legland, D., & Arganda-Carreras, I. (2016). Morpholibj User Manual. Institut National de la Recherche Agronomique: Nantes, France."]}

The present study aimed to assess the effectiveness of the image segmentation technique utilizing the Threshold method for the measurement of porosity in high-strength microconcrete samples that incorporate metakaolin. Specifically, X-ray microtomography testing was conducted on the microconcrete samples after 7 days of curing, and the voxel size was set at 20μm. Subsequently, the images were subjected to pre-processing measures including histogram regularization and noise reduction. Thereafter, the regions of interest within the images were demarcated through segmentation, enabling the isolation of the porosity from the other phases of the microconcrete. To execute the segmentation, grayscale values were systematically adjusted via the Threshold method to elucidate the impact of such variations on the determination of porosity properties. The study findings indicate that the proposed technique yields reliable measurements of the total porosity percentage of the material, despite the human factor inherent in the manual Threshold segmentation approach. However, caution should be exercised while performing segmentation when assessing pore quantity and dimensions as these are substantially influenced by this technique.

Published in International Journal of Advances in Engineering & Technology (IJAET), Volume 16 Issue 3, pp. 46-56, June 2023. Available at https://www.ijaet.org/media/1I75-IJAET1603601-v16-i3-pp46-56.pdf

Keywords

Threshold Method, X-Ray Microtomography, Microconcrete, Image Segmentation, Porosity Measurement, Metakaolin

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