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ZENODO
Dataset . 2023
License: CC BY
Data sources: Datacite
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ZENODO
Dataset . 2023
License: CC BY
Data sources: Datacite
image/svg+xml art designer at PLoS, modified by Wikipedia users Nina, Beao, JakobVoss, and AnonMoos Open Access logo, converted into svg, designed by PLoS. This version with transparent background. http://commons.wikimedia.org/wiki/File:Open_Access_logo_PLoS_white.svg art designer at PLoS, modified by Wikipedia users Nina, Beao, JakobVoss, and AnonMoos http://www.plos.org/
ZENODO
Dataset . 2023
License: CC BY
Data sources: ZENODO
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Claim

Crystal Structure Solution and High Temperature Thermal Expansions of NaZr2(PO4)3-type Materials

Research datakeyboard_double_arrow_right Dataset 06 Jul 2023 English Publisher:ZenodoFunded by:NSF | In situ Determination of ...
Authors: Benjamin Hulbert;

doi: 10.5281/zenodo.8121948 , 10.5281/zenodo.8121949

Crystal Structure Solution and High Temperature Thermal Expansions of NaZr2(PO4)3-type Materials

Abstract

The NaZr2P3O12 (NZP) family of materials have shown low and tailorable thermal expansion properties. This dataset includes SrZr4P6O24, CaZr4P6O24, NaTi2P3O12, NaZr2P3O12, MgZr4P6O24, and related solid solutions. These materials were synthesized using the organic-inorganic steric entrapment method. The samples were characterized with in-situ high-temperature x-ray diffraction at the Advanced Photon Source and National Synchrotron Light Source II from 25 to 1500 ℃. The average linear thermal expansion of SrZr4P6O24 and CaZr4P6O24 was between -1 x10-6/℃ and 6 x10-6/℃ from 25 to 1500 ℃. High temperature polymorphs of CaZr4P6O24 and SrZr4P6O24 were solved by Fourier difference mapping and Rietveld refinement. This polymorph is present above about 1250 ℃. This work measured thermal expansion coefficients to 1500 ℃ for all samples and investigated the differences in thermal expansion mechanisms between polymorphs and between compositions.

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Keywords

Crystal structure solution, SrZr4P6O24, NASICON, Fourier difference mapping, Powder XRD, CaZr4P6O24, crystallography, Phase transformation, NZP

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
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