Experimental data for the 'Chemically Reduced Graphene Oxide based Aerogels (rGOAs) - insight on the surface and textural functionalities dependent on handling the synthesis factors' manuscript/publication. Package contains following data: 1. File with description of the experimental conditions for rGOAs synthesis, format: .pdf, number of files: 1 2. Data of Boehm titration for graphene oxide used for synthesis of rGOAs, format: .txt, number of files: 12 3. Fourier-transform infrared spectra of rGOA samples and GO used for synthesis, format: .csv, number of files: 16 4. Raw chromatograms of test probes for rGOA samples, format .txt, number of files: 15 folder with 11 files in each