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ZENODO
Article . 1956
License: CC BY
Data sources: Datacite
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ZENODO
Article . 1956
License: CC BY
Data sources: Datacite
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STUDIES IN FRIES MIGRATION. PART XIII. FRIES REARRANGEMENT OF ACYL ESTERS OF METHYL 2 : 6-DTHYDROXYBENZOATE (METHYL γ-RESORCYLATE) AND 3 : 5 (DIHYDROXY- BENZOIC ACID (α-RESORCYLIC ACID)

descriptionPublicationkeyboard_double_arrow_right Article 30 Apr 1956 English Publisher:Zenodo
Authors: J. L. SETALVAD; G. C. AMIN; N. M. SHAH;

doi: 10.5281/zenodo.6565718 , 10.5281/zenodo.6565717

STUDIES IN FRIES MIGRATION. PART XIII. FRIES REARRANGEMENT OF ACYL ESTERS OF METHYL 2 : 6-DTHYDROXYBENZOATE (METHYL γ-RESORCYLATE) AND 3 : 5 (DIHYDROXY- BENZOIC ACID (α-RESORCYLIC ACID)

Abstract

The Fries rearrangement of methyl .2 : 6-diacetoxy- as well as -dibenzoyloxy-benzoate yields methyl 2 : 6-dihydroxy-3-acetyl- and -3 benzoyl-benzoates and the corresponding keto-acids respectively, hydro­lysis occurring during the course of the migration. No diketone has been isolated. 3 : 5-Diacetoxy benzoic acid does not isomerise under the conditions of the Fries reaction.

Keywords

Hydrolysis, Keto Acid, Benzoic Acid

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