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3D ED data of quartz, natrolite, CAP, abiraterone acetate, STW_HPM-1

Authors: Klar, Paul Benjamin; Krysiak, Yasar; Xu, Hongyi; Steciuk, Gwladys; Cho, Jung; Zou, Xiaodong; Palatinus, Lukas;

3D ED data of quartz, natrolite, CAP, abiraterone acetate, STW_HPM-1

Abstract

3D ED data of quartz, natrolite, cobalt aluminophosphate (CAP), and abiraterone acetate were measured with an FEI Tecnai G2 20 transmission electron microscope equipped with an Olympus SIS Veleta camera (CCD, 2048 x 2048 px) and a NanoMEGAS Digistar precession unit. One crystal of quartz and one crystal of natrolite were measured by stepwise continuous-rotation and precession-assisted 3D ED. Two crystals of CAP were measured in non-continous mode by recording static electron diffraction patterns every 0.1°. Five crystals of abiraterone acetate were measured in stepwise continuous-rotation 3D ED. STW_HPM-1 was measured at room temperature using a JEOL JEM-2100-LaB6 and diffraction patterns were recorded with an ASI Timepix detector. A different sample of STW_HPM-1 was measured after cryotransfer with a Titan Krios and diffraction patterns were recorded with a CETA-D detector. Each data set contains the raw diffraction patterns (*.tif) and the basic input files needed to reproduce the data reduction with PETS2 as used in the associated publication (*.pts2, *.celllist, *.cenloc). CIF (Crystallographic Information Framework) files based on the kinematical and dynamical refinements performed with JANA2006 are included.

CIF files are included for: - quartz (continuous-rotation) - natrolite (continuous-rotation) - CAP (static diffraction patterns) - abiraterone acetate (continuous-rotation) - STW_HPM-1 (continous-rotation, T = 100K)

Keywords

Dynamical refinement, 3DED, PETS2, JANA2006, cRED, MicroED

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
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