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ZENODO
Article . 1968
License: CC BY
Data sources: Datacite
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ZENODO
Article . 1968
License: CC BY
Data sources: ZENODO
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ZENODO
Article . 1968
License: CC BY
Data sources: Datacite
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Claim

Thermogravimetric Analysis (TGA) of the Sulphides of Selenium (IV), Tellurium (IV) and Vanadium (V) obtained with Potassium Thiocarbonate (PTC)

descriptionPublicationkeyboard_double_arrow_right Article 31 Oct 1968 English Publisher:Zenodo
Authors: N. K. Kaushik; K. N. Johri;

doi: 10.5281/zenodo.6472004 , 10.5281/zenodo.6472003

Thermogravimetric Analysis (TGA) of the Sulphides of Selenium (IV), Tellurium (IV) and Vanadium (V) obtained with Potassium Thiocarbonate (PTC)

Abstract

Unlike the conventional use of H2S as precipitant, potassium thiocarbonate (PTC) yields sulphides of selenium (IV), tellurium (IV) and vanadium (V) confirming to the stiochiometric composition of SeS2, TeS2 and V2S5, respectively. The procedure of precipitation in each case is based on the acidification of the thio­carbonato-complex, initially obtained with excess PTC. Thermogravimetric analysis (TGA) not only con­firms the purity of the precipitated products but determines correct temperature ranges for the precipitates to attain constant weight affording gravimetric estimation of Se, Te and V.

Keywords

Thermogravimetric Analysis, Selenium

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