This dataset contains the following profiles: Gunshot residue from Sellier & Bellot 9 mm Parabellum FMJ, Batch 4211/9 Gunshot residue from Sellier & Bellot 9 mm Parabellum, Batch 843 (old stock) Gunshot residue from Magtech 9 mm Parabellum LRN, Batch BA0916 L-93 Gunshot residue from Magtech Cleanrange 9 mm Parabellum JSP, Batch BA0910 L-01 Gunshot residue from CBC 9 mm Parabellum FMJ, Batch AQD518 L-430 (old stock) Propellant and gunshot residue from Eley Contact .22 Long Rifle Propellant and gunshot residue from Geco Rifle .22 Long Rifle Propellant and gunshot residue from Winchester Pistol .22 Long Rifle (old stock) Alliant Unique reloading propellant These profiles were obtained with GunShotMatch (https://doi.org/10.5281/zenodo.2669156) following Gas Chromatography-Mass Spectrometry