The synthesis of heterocyclic compounds especially when their structure containing nitrogen ,oxygen and sulfur atoms are growing up due to their wide spread in nature ,many mechanistic pathways to reach the target with nearly negligible loss of their dose and there are numerous me thods to derivatives their structures There for the development in hetero cyclic synthesis will provide new metabolic pathways when these compounds have succeeded to be used as drug ,Moreover it was known for long time that about 95 % of cancer drugs are heterocyclic compounds .There are also many methods found in the literature for the synthesis of both triazoles and trdiazines from different routes In this investigation furfural was used as precursor for the synthesis of some new diazine and triazole derivatives (3-11).The synthesized compounds were characterized by IR ,and 1HNMR and are discussed.