This dataset contains the raw and processed analytical data used to characterize carbohydrate fractions and the fiber profile of Hyphaene coriacea Gaertn. The dataset was prepared to support transparency, traceability, and reusability of the analytical results. It provides the underlying values used for the determination and interpretation of carbohydrate-related components and fiber fractions of Hyphaene coriacea Gaertn. The files are organized to facilitate verification of results, secondary analysis, and citation of the dataset as a standalone research output. Files included:- Data workbook ;- Analytical data ;- Readme.