Dataset for "Glue-assisted Exfoliation of Two-dimensional Sulfur-rich Niobium Thiophosphate (Nb4P2S21) for Sulfur-equivalent Electrode Study in Lithium Storage" The dataset contains all relevant data and figures regarding the manuscript "Glue-assisted Exfoliation of Two-dimensional Sulfur-rich Niobium Thiophosphate (Nb4P2S21) for Sulfur-equivalent Electrode Study in Lithium Storage". All Figures are in tiff format and all relevant data are in csv formats. The data in csv format are labelled as specified in the corresping images (e.g. Figure 1a csv file corresponds to data used to plot graphs from Figure 1a etc.). Axis labeling and units are always specified at the beginning of individual columns. If more than one curve was plotted from the csv file, the conditions can also be found at the beginning of corresponding columns.