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In this work, we present an easy synthesis of a alternative precursor for CVD of parylene AF-4 to the widely used standard, Octafluoro[2.2]paracyclophane. The standard precursor suffers from uncertainties in its supply chain and its synthesis is of low yield. A comparison between different reaction parameters and solvents are being discussed by means of thermal, laboratory scale and microwave assisted reactions and qNMR studies.
Usage notes are included in the .zip-file. File name: "Interpretation of spectroscopic data"
There is GC-MS data available, as well as infrared and various NMR spectra.
FOS: Chemical sciences, parylene, precursor, CVD
FOS: Chemical sciences, parylene, precursor, CVD
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