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Дилатометрическое исследование критических точек стали 13Х11Н2В2МФ

Authors: Mirzaev, D.A.; Mirzoev, A.A.; Sozykin, S.A.; Vorob'eva, A.S.;

Дилатометрическое исследование критических точек стали 13Х11Н2В2МФ

Abstract

Д.А. Мирзаев, А.А. Мирзоев, С.А. Созыкин, А.С. Воробьева, Южно-Уральский государственный университет, г. Челябинск, Российская Федерация E-mail: mizaevda@susu.ru. D.A. Mirzaev, A.A. Mirzoev, S.A. Sozykin, A.S. Vorob'eva South Ural State University, Chelyabinsk, Russian Federation E-mail: mizaevda@susu.ru При скоростях нагрева и охлаждения до 30 °С/мин записаны дилатограммы для различных режимов термической обработки высокопрочной мартенситной стали 13Х11Н2В2МФ и определены её важнейшие критические точки. При малых скоростях нагрева температура образования аустенита AC1 составляет 750 °С, однако её положение зависит от скорости нагрева и однородности состава образцов по объёму и может достигать 810 °С. Показано, что существенное влияние на мартенситную точку исследуемой стали оказывает температура начала охлаждения, длительность выдержки и наличие температурных остановок, если они сопровождаются выделением из аустенита карбидных частиц. Второй использованный в исследовании метод измерения AC1 основан на анализе графика зависимости твёрдости образцов закалённой стали от температуры отпуска при фиксированной длительности отпуска (2 ч). Пока температура выдержки не превысит AC1, в образцах проходят процессы, приводящие к снижению твердости. Однако как только повышаемая температура переходит через критическую точку, наряду с отпуском сохранившегося мартенсита начинается образование кристаллов аустенита, что после резкого охлаждения в воде вновь приводит к повышению твёрдости. Поэтому минимум твёрдости соответствует температуре AC1. Этот метод дал такой же результат, что и дилатометрия, AC1 = 750 °С. At the heating and cooling rates up to 30 °C/min, dilatograms for different heat treatment regimes for high-strength martensitic 13X11N2V2MF steel are recorded, and its critical points are determined. At low heating rates, the temperature of formation of austenite AC1 is 750 °C, but its position depends on the heating rate and uniformity of the sample composition in volume, and can reach 810 °C. It is shown that the temperature of the beginning of cooling, the duration of soaking and the presence of temperature stops, if they are accompanied by the release of carbide particles from the austenite, have a significant effect on the martensitic point of the steel under study. The second method of measurement AC1 used in the study is based on the analysis of the dependence of the hardness of hardened steel samples on the tempering temperature for a fixed duration of tempering (2 hours). As long as the holding temperature does not exceed AC1, processes lead to a decrease in hardness in the samples. However, once the elevated temperature passes through the critical point, along with the tempering of the preserved martensite, the formation of austenite crystals begins, which, after abrupt cooling in water, again leads to an increase in hardness. Therefore, the minimum hardness corresponds to the temperature of AC1. This method gave the same result: AC1 = 750 °C, which is the same as dilatometry. Исследование выполнено при поддержке гранта Российского научного фонда № 16-19- 10252.

Keywords

механические свойства, martensitic transition, дилатометрическое исследование, УДК 538.951, мартенситное превращение, сталь 13Х11Н2В2МФ, mechanical properties, 13X11N2V2MF steel, dilatometric study

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
0
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