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Nuclear Instruments and Methods in Physics Research, Section A: Accelerators, Spectrometers, Detectors and Associated Equipment

Authors: Stahn, J.; Glavic, A.;

Nuclear Instruments and Methods in Physics Research, Section A: Accelerators, Spectrometers, Detectors and Associated Equipment

Abstract

Neutron reflectometry is a powerful tool to investigate chemical and magnetic depth profiles near surfaces. The advantages of neutrons compared to x-rays are their sensitivity to isotopes, the high penetration capabilities and the high sensitivity to magnetic induction. The biggest disadvantage however is the low flux available, which leads to much longer counting times on much larger samples. In order to boost the performance of neutron reflectometers, a focusing guide system was developed and realised over recent years. Here we report on the application and performance of a down-scaled demonstrator of such Selene guide, installed as an add-on on the time-of-flight (TOF) reflectometer Amor at the PSI. Due to the limited size of the guide, the flux is concentrated to a footprint of at most 2 mm width. It is thus possible to avoid illumination of contacts even on small samples. Despite the fact that typical samples measured on Amor with a size of 10 x 10 mm2 are markedly under illuminated, the presented set-up leads to a reduction in counting time of 80%. The use of the demonstrator thus allows for in-situ or in-operando investigations with a time resolution of a few minutes for a qz range from 0.005 Å-1 to 0.08 Å-1. Besides a short recapitulation of the concept of focusing reflectometry, a detailed description of the data reduction and its quality is given, followed by an application example.

Country
Switzerland
Related Organizations
Keywords

focusing, reflectometry, neutron

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
0
Average
Average
Average