Chitosan from prawn waste was used for the removal of mercury from solutions. Mercuric chloride solutions containing 250, 500, 1000, 10000 and 100000 ng of Hg super(+2)/ml were treated with chitosan samples of different particle size for different periods. The effect of initial concentration of mercury in the solution, particle size of chitosan and time of treatment on the adsorption of Hg super(+2) was studied. The residual mercury content after treatment for ten min. with chitosan of 40 mesh size from a solution of initial concentration 10000 ng/ml was 10 ng/ml whereas it was 50 ng/ml for chitosan of larger particle size (10-20 mesh). From solutions of lower concentrations complete removal of mercury was possible by chitosan treatment. Though the particle size and time of treatment have significant effect, the concentration of mercury in solution is more influential on the removal of mercury from solution.