[Determination of cirsilineol in Herba Artemisiae scopariae collected in autumn by HPLC].
Copyright policy )[Determination of cirsilineol in Herba Artemisiae scopariae collected in autumn by HPLC].
To establish a quantitative method for determination of cirsilineol in Herba Artemisiae Scopariae collected in Autumn.Sample was extracted with methanol, and cleaned up with polyamide column. ODS column was used with methanol-acetonitrile-0.5% acetic acid solution (24:19:57) as mobile phase. Detection wavelength was 347 nm.Cirsilineol in sample solution was well separated. Linearity of cirsilineol was good (r = 0.9998) in range of 0.1-0.8 microgram. The average recovery was 101.3%, RSD of repeatability was 3.04%.This method can be used for quality control of Herba Artemisiae Scopariae collected in autumn and its preparations.
- Institute of Chinese Materia Medica China (People's Republic of)
Flavonoids, Quality Control, Plants, Medicinal, Artemisia, Seasons, Flavones, Chromatography, High Pressure Liquid
Flavonoids, Quality Control, Plants, Medicinal, Artemisia, Seasons, Flavones, Chromatography, High Pressure Liquid
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