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Sammenlignende laboratorieprøvninger (SLP) – Analyse av ferskvann. SLP 15-24

Authors: Bryntesen, Tina; Blakseth, Tomas Adler;

Sammenlignende laboratorieprøvninger (SLP) – Analyse av ferskvann. SLP 15-24

Abstract

Under en sammenlignende laboratorieprøvning (SLP) gjennomført i november desember 2015 bestemte 54 laboratorier pH, konduktivitet, turbiditet, farge, UV-absorpsjon, natrium, kalium, kalsium, magnesium, hardhet, alkalitet, klorid, sulfat, fluorid, totalt organisk karbon, kjemisk oksygenforbruk (CODMn), fosfat, totalfosfor, ammonium, nitrat, totalnitrogen, aluminium, bly, jern, kadmium, kobber, krom, mangan, nikkel, sink, antimon og arsen i vann. Prøvene ble laget ved å tilsette kjente stoffmengder til vann fra Glomma og Damtjern i Aurskog-Høland kommune. Vannet var på forhånd filtrert gjennom membranfilter med porevidde 0,45 µm. Totalt ble 82 % av resultatene vurdert som akseptable, en andel som er noe høyere enn det foregående år og litt over det gjennomsnittlige nivået for disse SLPene. Best resultater viser natrium, kalium, kalsium, magnesium, og jern. Alle disse hadde en andel akseptable resultater over 90 %. De svakeste resultater ble observert for ammonium, nitrat (i ukonserverte prøver), totalnitrogen, kadmium og arsen. Alle disse hadde mindre enn 70 % akseptable resultater. En del av parameterne opptrådte dessuten i lave konsentrasjoner og laboratoriene må ta hensyn til usikkerheten i "sann verdi" ved evalueringen av sine resultater. Det er stor variasjon i analysekvaliteten mellom laboratoriene, og de som har avvikende resultater bør snarest vurdere disse resultater opp mot egne oppgitte analyseusikkerheter for de aktuelle analysene og deretter eventuelt igangsette tiltak for å forbedre kvaliteten på bestemmelsene.

The 24th Norwegian intercomparison study for analysis of fresh water, designated 15-24, was organized in November-December 2015 with 54 participants. It comprised analysis of three sample sets of four samples (A-D, E-H, I-L), and two sample sets of two samples (M-N and O-P), made by adding known amounts of stoichiometric material to water from the river Glomma and Damtjern in Aurskog-Høland municipality, which had been filtered through membrane filter with pore size 0,45 µm. The program included 32 different parameters: pH, conductivity, turbidity, colour, UV-absorption, sodium, potassium, calcium, magnesium, hardness, alkalinity, chloride, sulfate, fluoride, total organic carbon, chemical oxygen demand (CODMn), phosphate, total phosphorus, ammonium, nitrate, total nitrogen, aluminium, lead, iron, cadmium, copper, chromium, manganese, nickel, zinc, antimony and arsenic. The analysis was largely carried out according to Norwegian standards or equivalent methods (Table B1).

NIVA

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Norway
Related Organizations
Keywords

Prestasjonsprøving / Profiency testing, Akkreditering / Accreditation, Ferskvannsanalyse / Freshwater analysis, VDP::Matematikk og naturvitenskap: 400, SLP / Interlaboratory comparison, VDP::Mathematics and natural scienses: 400

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
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