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Částicové kompozity vyztužené krátkými vlákny

Authors: Kročová, Blanka;

Částicové kompozity vyztužené krátkými vlákny

Abstract

This diploma thesis examines the effect of short fiber reinforcement in particle composite with a polymer matrix and the effect of its structure on the mechanical properties. It studies the refraction toughness depending on the addition of short polyvinylalcohol fibers (PVAL), nanosilica and pulverized polymethylacrylate (PMMA) to a dimethylacrylate matrix. Matrix strengthening was characterised with the help of differential compensation photocalorimetry. The inner structure of the composite and the morphology of fracture were studied using a scanning electron microscope. For the tested samples, the modules of elasticity and toughness were measured, the critical values of stress intensity factor and the energy release rate were determined. The findings suggest that the limit value of short fibers content is 4 vol. %. This content of fibers significantly increases the tenacity of the material but at the same time the uniform distribution of fibers and the ease of preparation of the material decrease. Within the possible applications, the manipulation of this material worsens as well. The fibers content of 2 ± 0.5 vol. % is an acceptable compromise between good treatability, uniform distribution of fibers and the required mechanical properties. During the study of the fracture surfaces of the material, different types of fibers disruption were witnessed (extraction from the matrix, plastic deformation, fibrillation on the surface of the fibers, fracture) depending on the type of used matrix and filling.

Tato diplomová práce zkoumá vliv vyztužení krátkých vláken v částicovém kompozitu s polymerní matricí a vliv jeho struktury na mechanické vlastnosti. Studuje lomovou houževnatost v závislosti na přídavku krátkých polyvinylalkoholových (PVAL) vláken, nanosiliky a práškového polymethylmethakrylátu (PMMA) do dimethakrylátové matrice. Vytvrzování matric bylo charakterizováno pomocí diferenční kompenzační fotokalorimetrie. Vnitřní struktura kompozitu a morfologie lomu byla studována s použitím skenovacího elektronového mikroskopu. U testovaných zkušebních vzorků byly změřeny moduly pružnosti, pevnosti a stanoveny kritické hodnoty faktoru intenzity napětí a rychlosti uvolňování energie. Ze získaných poznatků vyplývá, že limitní hodnotou obsahu krátkých vláken jsou 4 obj. %. Při tomto obsahu vláken se sice významně zvýší houževnatost materiálu, ale zároveň se sníží rovnoměrná distribuce vláken a snadnost přípravy materiálu. V rámci možných aplikací se také zhorší manipulovatelnost s tímto materiálem. Obsah vláken 2 ± 0,5 obj. % je přijatelným kompromisem mezi dobrou zpracovatelností, rovnoměrnou distribucí vláken a požadovanými mechanickými vlastnostmi. Při studiu lomových ploch materiálu docházelo k různým porušením vláken (vytahování z matrice, plastická deformace, fibrilace na povrchu vláken, lom) v závislosti na typu použité matrice a plniva.

A

Country
Czech Republic
Related Organizations
Keywords

hybrid composite, lomová houževnatost, dental materials, short fibers, krátká vlákna, dentální materiály, hybridní kompozity, fracture toughness

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
0
Average
Average
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