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handle: 10261/67468
Se han obtenido materiales compuestos de A^Oyplaquetas de SiC mediante tres vías de sinterización diferentes: prensado en caliente, sinterización convencional y sinterización bajo presión de gas. El objetivo fundamental ha sido el estudio del efecto de las condiciones de procesado en el grado de densificación y la microestructura de estos materiales. Las mezclas perfectamente homogéneas de AI2O3/SÍC con contenidos en plaquetas del 5 y 12 % en volumen se ha preparado mediante floculación instantánea de las correspondientes suspensiones estables. Se han conseguido materiales con densidades próximas a la teórica utilizando prensado en caliente a 1500-1550 "C en atmósfera de argón. Sin embargo, esta técnica sólo permite la fabricación de piezas con geometrías muy simples que requieren un mecanizado posterior, por lo que se han considerado otras vías de sinterización (convencional y bajo presión de gas) que permiten desarrollar componentes con formas cercanas a las necesarias para sus aplicaciones fínales. Aunque las densidades obtenidas usando estas vías son menores que las correspondientes al prensado en caliente, con el método de sinterización bajo presión de gas se alcanzan densidades aceptables, cercanas al 97 % de la teórica.
AI2O3/SÍC platelets composites have been obtained by three different sintering routes: hot pressing, pressureless sintering and gas pressure sintering. The main objective of this work has been to study the effect of processing parameters on the densifîcation and microstructure of these materials. Highly homogeneous mixtures of AI2O3/SÍCwith different platelets content (5 and 12 %) have been prepared by instantaneous flocculation of the stable suspensions. For the compacts obtained by hot pressing, at 1500- 1550 "C in argon atmosphere, relative densities very close to theoretical value have been achieved. However, this technique only allows the fabrication of pieces with simple geometry that require extensive machining, and therefore other sintering routes (pressureless and gas pressure sintering) which can be used to develop nearnet-shape components have been considered. Although the relative densities obtained by these sintering routes are lower than those for hot pressed composites, relative densities close to 97 % of the theoretical have been reached using gas pressure sintering
Peer reviewed
plaquetas, Procesamiento
plaquetas, Procesamiento
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