Sodium borohydride-amberlyst-15 (H+): An effective reductor for hindered and unreactive ketones in aprotic solvent

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1997 Spain English Publisher:Elsevier BVJournal:Tetrahedron Letters, volume 38, pages 277-280 (issn: 0040-4039,

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Authors: Juana Robles Caycho; Fernando García Tellado; Pedro de Armas; José Juan; Marrero Tellado;

doi: 10.1016/s0040-4039(96)02291-5

handle: 10261/132687

Sodium borohydride-amberlyst-15 (H+): An effective reductor for hindered and unreactive ketones in aprotic solvent

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Abstract

The combination of sodium borohydride and amberlyst-15 (H+) in tetrahydrofurane is a powerful reductor for unreactive ketones. The reduction is fast, high-yielding and the work-up is extremely simple. Ketals, silyl ethers and other organic functions are not disturbed during the reduction.

This work was supported by the Spanish DGICYT (PB94-0028). JRC thanks the ICI for a predoctoral fellowship.

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Spain

Related Organizations

Spanish National Research Council
Spain
University of La Laguna
Spain
Instituto de Productos Naturales y Agrobiología
Spain

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