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Synthesis Methods in Solid-State Chemistry

طرق التوليف في كيمياء الحالة الصلبة
Authors: Youssef Ben Smida; Riadh Marzouki; Savaş Kaya; Sultan Erkan; Mohamed Faouzi Zid; Ahmed Hichem Hamzaoui;

Synthesis Methods in Solid-State Chemistry

Abstract

La synthèse du monocristal est un domaine d'activité intense dans la science des matériaux. L'obtention du monocristal avec une dimension suffisante pour la diffraction des rayons X dépend de plusieurs facteurs, notamment la composition chimique, la structure cristalline des réactifs et les paramètres physiques (température et pression). Dans ce contexte, ce chapitre est consacré à la description des méthodes de synthèse les plus courantes du monocristal dans la chimie à l'état solide : méthode à l'état solide, hydrothermale et évaporation lente à température ambiante. Même d'autres matériaux peuvent être obtenus à haute pression. Il existe également des techniques physiques pour faire croître le monocristal, chaque technique est spécifique à des matériaux spécifiques.

La síntesis del monocristal es un área de intensa actividad en la ciencia de los materiales. La obtención del monocristal con dimensión suficiente para la difracción de rayos X depende de varios factores, entre ellos la composición química, la estructura cristalina de los reactivos y los parámetros físicos (temperatura y presión). En este contexto, este capítulo está dedicado a la descripción de los métodos de síntesis más comunes del monocristal en la química de estado sólido: método de estado sólido, hidrotermia y evaporación lenta a temperatura ambiente. Los mismos otros materiales se pueden obtener a alta presión. También hay algunas técnicas físicas para cultivar monocristales, cada técnica es específica para materiales específicos.

The synthesis of single crystal is an area of intense activity in the materials science.The obtaining of the single crystal with sufficient dimension for X-ray diffraction depends on several factors including the chemical composition, crystal structure of the reagents, and physical parameters (temperature and pressure).In this context, this chapter is dedicated to the description of the most common synthesis methods of single crystal in the solid-state chemistry: solid-state method, hydrothermal, and slow evaporation at room temperature.Same other materials can be obtained at high pressure.There are also some physical techniques to grow single crystal, each technique is specific for specific materials.

يعد تركيب البلورة المفردة مجالًا من النشاط المكثف في علم المواد. يعتمد الحصول على البلورة المفردة ذات البعد الكافي لحيود الأشعة السينية على عدة عوامل بما في ذلك التركيب الكيميائي والبنية البلورية للكواشف والمعلمات الفيزيائية (درجة الحرارة والضغط). في هذا السياق، يخصص هذا الفصل لوصف طرق التركيب الأكثر شيوعًا للبلورة المفردة في كيمياء الحالة الصلبة: طريقة الحالة الصلبة والحرارة المائية والتبخر البطيء في درجة حرارة الغرفة. يمكن الحصول على نفس المواد الأخرى عند الضغط العالي. هناك أيضًا بعض التقنيات الفيزيائية لزراعة بلورة مفردة، كل تقنية محددة لمواد محددة.

Keywords

Materials Science, Evaporation, Catalytic Dehydrogenation of Light Alkanes, Hydrothermal circulation, Crystal (programming language), Catalysis, Context (archaeology), Chemical engineering, Engineering, FOS: Chemical sciences, Solid-state, Materials Chemistry, Reagent, Nanotechnology, Hydrothermal synthesis, Kinetic Analysis of Thermal Processes in Materials, FOS: Chemical engineering, FOS: Nanotechnology, Crystallography, Single crystal, Crystal structure, Physics, Organic Chemistry, Paleontology, Geology, Solid-state chemistry, FOS: Earth and related environmental sciences, Chemical Engineering, Organic Chemistry and Catalysis, Computer science, Materials science, Programming language, Chemistry, Heterogeneous Catalysis, Physical chemistry, Physical Sciences, Thermodynamics, Crystal chemistry

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
8
Top 10%
Average
Average
hybrid