Coconut toddy is an effervescence beverage tapped from young inflorescence of coconut tree, Cocos nucifera. The sap contains various nutrients, though it undergoes natural fermentative changes when it is stored. The physicochemical changes like pH, turbidity, acidity, alcohol content, total sugars, and total soluble solid, reducing sugar and non reducing sugar occurs in toddy on storage were analyzed. The toddy pH changed to 4.21 from 5.5 and the titratable acidity increased from 0.75 to 0.91 on storage. The lowest alcohol content of 0.2% was observed in fresh toddy which further increased to 4.5% on storage. The ash and ascorbic acid content of 0.12% and 5.8 mg/100ml found in fresh toddy increased to 0.38% and 3.5ml/ ml respectively. Whereas the total carbohydrates content of 66 mg/100 ml reduced to 40 mg/100ml after 24 hours storage.