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Polymers
Article . 2021 . Peer-reviewed
License: CC BY
Data sources: Crossref
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Polymers
Article
License: CC BY
Data sources: UnpayWall
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PubMed Central
Other literature type . 2021
License: CC BY
Data sources: PubMed Central
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Usage of Near-Infrared Spectroscopy for Inline Monitoring the Degree of Curing in RTM Processes

Authors: Moritz Salzmann; Yannick Blößl; Andrea Todorovic; Ralf Schledjewski;

Usage of Near-Infrared Spectroscopy for Inline Monitoring the Degree of Curing in RTM Processes

Abstract

Near-infrared spectroscopy (NIR) was implemented in the resin transfer molding (RTM) process to inline monitor the degree of curing of a bio-based epoxy resin, which consists of epoxidized linseed oil (resin) and citric acid (hardener), respectively. A NIR micro-spectrometer was used for the development of robust calibration models using partial least squares (PLS) regression. Since the micro-spectrometer offers a smaller wavelength range compared with conventional NIR devices, and typical absorbance peaks are not directly involved in the captured data range, the results show new insights for the utilization of this technology. Different pre-treatments of the spectroscopic data have been tested, starting with different reference spectra, i.e., uncured resin and polytetrafluorethylene (PTFE), and followed by chemometrical algorithms. As a reference method for the degree of curing, direct current (DC) supported by differential scanning calorimetry (DSC) was used. The results show the potential of these cost-efficient and compact NIR micro-spectrometers for the intended inline monitoring purpose to gain relevant information feedback during the process.

Keywords

near-infrared spectroscopy (NIR), epoxy-resin, inline monitoring, resin transfer molding (RTM), Article

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
10
Top 10%
Average
Top 10%
Green
gold