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Crystal Structure and Hirshfeld Surface Analysis of Acetoacetanilide Based Reaction Products

descriptionPublicationkeyboard_double_arrow_right Article , Other literature type 09 May 2020 English Publisher:MDPI AGJournal:Molecules, volume 25, page 2,235 (eissn: 1420-3049, Copyright policy )
Authors: Farid N. Naghiyev; Jonathan Cisterna; Ali N. Khalilov; Abel M. Maharramov; Rizvan K. Askerov; Khammed A. Asadov; Ibrahim G. Mamedov; +3 Authors

doi: 10.3390/molecules25092235

pmid: 32397450

pmc: PMC7248728

Crystal Structure and Hirshfeld Surface Analysis of Acetoacetanilide Based Reaction Products

Abstract

We report an unprecedented multicomponent reaction of acetoacetanilide with malononitrile leading to a structurally novel bicyclic product (9) in a high yield. The structure has been confirmed by X-ray crystallography and comparative Hirshfeld surface analysis of 5-cyano-2-hydroxy-2-methyl-N-phenyl-4-(yridine-4-yl)-6-(thiophen-2-yl)-3,4-dihydro-2H-pyran-3-carboxamide 2, 5-cyano-2-hydroxy-2-methyl-6-oxo-N-phenyl-4-(thiophen-2-yl)piperidine-3-carboxamide 4 and 2-(8-amino-7,8a-dicyano-1-imino-4a-methyl-3-oxo-2-phenyl-1,3,4,4a,5,8a-hexahydroisoquinolin-6(2H)-ylidene)-N-phenylacetamide 9.

Related Organizations
Keywords

multicomponent reaction, Molecular Structure, Surface Properties, Organic chemistry, acetoacetanilide, Crystallography, X-Ray, Article, Structure-Activity Relationship, QD241-441, Hirshfeld surface analysis, Acetanilides, X-ray analysis

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
24
Top 10%
Top 10%
Top 10%
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