
doi: 10.3390/m1924
handle: 11584/429745 , 10023/30965
Ammonium oxathioamidate (1) was synthesised by the reaction between O-ethyl-thioxamate (oxalic acid-1-amide-2-O-ethyl ester) and ammonium hydrogen carbonate in water solution. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single-crystal X-ray diffraction were isolated by slow evaporation of an ethanol solution of the compound. The analysis of the crystal packing reveals the prominent role exerted by intermolecular hydrogen bonding (HB) and chalcogen bonding (ChB) interactions.
Hydrogen bonding, MCC, oxalic acid derivatives, XRD, DAS, 540, Oxalic acid derivatives, QD Chemistry, hydrogen bonding, Thiooxamate, hydrogen bonding; oxalic acid derivatives; thiooxamate; XRD, QD, thiooxamate, Inorganic chemistry, QD146-197
Hydrogen bonding, MCC, oxalic acid derivatives, XRD, DAS, 540, Oxalic acid derivatives, QD Chemistry, hydrogen bonding, Thiooxamate, hydrogen bonding; oxalic acid derivatives; thiooxamate; XRD, QD, thiooxamate, Inorganic chemistry, QD146-197
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