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Annals of the Missouri Botanical Garden
Article
License: CC BY NC SA
Data sources: UnpayWall
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Annals of the Missouri Botanical Garden
Article . 1926 . Peer-reviewed
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Determination of Total Nitrogen, Nitrate-Nitrogen, and Total Nitrogen not Including Nitrate-Nitrogen: Further Observations on a Modification of the Official Salicylic-Thiosulphate Method

Authors: Ranker, Emery R;

Determination of Total Nitrogen, Nitrate-Nitrogen, and Total Nitrogen not Including Nitrate-Nitrogen: Further Observations on a Modification of the Official Salicylic-Thiosulphate Method

Abstract

The data here presented are in continuation of a series of investigations previously reported (Ranker, '25). These previous data were presented in support of a proposed modification of the official salicylic-thiosulphate method for the determination of total nitrogen including nitrate-nitrogen. BThe recommended procedure is as follows: "Place the sample in an 800-cc. Kjeldahl flask; adjust to neutrality or make slightly alkaline; if water is present evaporate just to dryness on a water bath under vacuum. Add 35-40 cc. of salicylic acid mixture (1.0 gm. of salicylic acid to 30 cc. of concentrated nitrogenfree sulphuric acid); mix thoroughly and allow to stand for at least an hour with occasional shaking (if organic matter is present, stopper tightly with a rubber cork and allow to stand over night). Add 5 gms. of sodium thiosulphate and heat for 5 minutes with a low flame; cool; add 7-10 gms. of anhydrous sodium sulphate and a pinch of copper sulphate. Digest for an hour at the boiling point after the solution clears; just before the solution solidifies dilute to an estimated volume of 400 cc.; cool completely. Add a small piece of paraffin, 100 cc. of a saturated solution of sodium hydroxide, and a piece of

Keywords

Source: Biodiversity Heritage Library, Source: BHL, Biodiversity, BHL-Corpus, Source: https://biodiversitylibrary.org

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
0
Average
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