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Metallographic preparation of titanium diboride coatings

Authors: McAllaster, Mark E.;

Metallographic preparation of titanium diboride coatings

Abstract

A method is described for preparing metallographic cross sections of thin, hard, chemically vapor deposited titanium diboride coatings on various softer substrates. Standard metallographic preparation techniques were found to result in fracturing and edge rounding of the coatings. It is shown that these problems can be avoided by unidirectional grinding on worn 600 grit silicon carbide abrasive paper. Typical photomicrographs of chemically vapor deposited titanium diboride coatings are shown along with photomicrographs of intermediate phases that form at the titanium diboride - substrate interfaces.

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United States
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Keywords

Boron Compounds, And Peat, Tokamak Type Reactors, Failures, Titanium Compounds, Borides, Iron Base Alloys, Chemical Coating, Iron Alloys, Thermochemical Processes, Alloys, 700209 -- Fusion Power Plant Technology-- Component Development & Materials Testing, Comminution, Lignite, Copper Alloys, Deposition, 010404 -- Coal, & Refractories-- Physical Properties, Silicon Carbides, Surface Finishing, Polishing, Substrates, Titanium Borides, Grinding, 36 Materials Science, Silicon Compounds, Thermonuclear Reactors, Elements, Machining, Carbon, Carbon Compounds, Transition Element Compounds 360204* -- Ceramics, 01 Coal, Coal Gasification, Chemical Vapor Deposition, Nonmetals, Erosion, Nickel Alloys, Metallography, Cermets, Graphite, Surface Coating, 70 Plasma Physics And Fusion Technology, Steels, Carbides, Fractures, Gasification, & Peat-- Gasification

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
0
Average
Average
Average