
doi: 10.1557/proc-9-533
ABSTRACTPreviously we reported on a theoretical treatment of the influence on freezing rate of sudden changes in translation rate in the Bridgman-Stockbarger technique [11]. This has now been extended to consideration of a linear ramped translation rate and an oscillatory freezing rate. Oscillations above a few hertz are found to be highly damped in smalldiameter apparatus.An experimental test was made of the theoretical predictions for a sudden change of translation rate. MnBi-Bi eutectic was solidified with current induced interface demarcation.The experimental results correspond reasonably well with theory if the silica ampoule wall is assumed either (1) to contribute only a resistance to heat exchange of sample with the furnace wall, or (2) to transmit heat effectively in the axial direction by radiation.In an attempt to explain the fact that a finer microstructure is obtained in space, MnBi-Bi microstructure is being determined when the freezing rate is rapidly increased or decreased. Preliminary results indicate that fiber branching does not occur as readily as does fiber termination.
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