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image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Journal of Materials...arrow_drop_down
image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao
Journal of Materials Research
Article . 2006 . Peer-reviewed
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Contact creep compliance of viscoelastic materials via nanoindentation

Authors: Catherine A. Tweedie; Krystyn J. Van Vliet;

Contact creep compliance of viscoelastic materials via nanoindentation

Abstract

The creep compliance of viscoelastic materials such as synthetic polymers is an established metric of the rate at which strain increases for a constant applied stress and can, in principle, be implemented at the nanoscale to compare quantitatively bulk or thin film polymers of different structures or processing histories. Here, we outline the evolution of contact creep compliance analysis and application for both conical and spherical indenter geometries. Through systematic experiments on four amorphous (glassy) polymers, two semi-crystalline polymers and two epoxies, we show that assumptions of linear viscoelasticity are not maintained for any of these polymers when creep compliance is measured via conical indentation at the nanoscale, regardless of the rate of stress application (step or ramp). Further, we show that these assumptions can be maintained to evaluate the contact creep complianceJc(t) of these bulk polymers, regardless of the rate of stress application, provided that the contact strains are reduced sufficiently through spherical indentation. Finally, we consider the structural and physical properties of these polymers in relation toJc(t), and demonstrate thatJc(t) correlates positively with molecular weight between entanglements or crosslinks of bulk, glassy polymers.

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
182
Top 1%
Top 1%
Top 1%
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