Tri(hetero)substituted Carbonium Ions. XI. A Novel Synthetic Route to 2-Dialkylamino-4-alkyl-1,3-dithiolium Salts

descriptionPublicationkeyboard_double_arrow_right Article 01 Mar 1976 English Publisher:Oxford University Press (OUP)Journal:Bulletin of the Chemical Society of Japan, volume 49, pages 827-828 (issn: 0009-2673, eissn: 1348-0634,

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Authors: Takeshi Nakai; Kazuhisa Hiratani; Makoto Okawara;

doi: 10.1246/bcsj.49.827

Tri(hetero)substituted Carbonium Ions. XI. A Novel Synthetic Route to 2-Dialkylamino-4-alkyl-1,3-dithiolium Salts

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Abstract

Abstract Pyrolysis of 2-dialkylamino-4-(α-bromoalkyl)-1,3-dithiolanylium bromides (2) readily prepared by bromination of the β,γ-unsaturated dithiocarbamates (1) affords 2-dialkylamino-4-alkyl-1,3-dithiolium salts (3) in good yields, providing a useful way to prepare dithiolium salts.

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Institute of Science Tokyo
Japan

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