
We report the results of a comparative study of the magnetic microstructure of textured and isotropic $\mathrm{Nd}_2\mathrm{Fe}_{14}\mathrm{B}/α$-$\mathrm{Fe}$ nanocomposites using magnetometry, transmission electron microscopy, synchrotron x-ray diffraction, and, in particular, magnetic small-angle neutron scattering (SANS). Analysis of the magnetic neutron data of the textured specimen and computation of the correlation function of the spin misalignment SANS cross section suggests the existence of inhomogeneously magnetized regions on an intraparticle nanometer length scale, about $40-50 \, \mathrm{nm}$ in the remanent state. Possible origins for this spin disorder are discussed: it may originate in thin grain-boundary layers (where the materials parameters are different than in the $\mathrm{Nd}_2\mathrm{Fe}_{14}\mathrm{B}$ grains), or it may reflect the presence of crystal defects (introduced via hot pressing), or the dispersion in the orientation distribution of the magnetocrystalline anisotropy axes of the $\mathrm{Nd}_2\mathrm{Fe}_{14}\mathrm{B}$ grains. X-ray powder diffraction data reveal a crystallographic texture in the direction perpendicular to the pressing direction -- a finding which might be related to the presence of a texture in the magnetization distribution, as inferred from the magnetic SANS data.
Physical, chemical, mathematical & earth Sciences, Condensed Matter - Mesoscale and Nanoscale Physics, Physique, chimie, mathématiques & sciences de la terre, Mesoscale and Nanoscale Physics (cond-mat.mes-hall), FOS: Physical sciences
Physical, chemical, mathematical & earth Sciences, Condensed Matter - Mesoscale and Nanoscale Physics, Physique, chimie, mathématiques & sciences de la terre, Mesoscale and Nanoscale Physics (cond-mat.mes-hall), FOS: Physical sciences
| selected citations These citations are derived from selected sources. This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically). | 12 | |
| popularity This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network. | Average | |
| influence This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically). | Average | |
| impulse This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network. | Top 10% |
