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image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao https://doi.org/10.1...arrow_drop_down
image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao
https://doi.org/10.1103/physre...
Article . 1939 . Peer-reviewed
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On the Single Crystal X-Ray Diffraction Pattern of Calcite

Authors: Franklin Miller;

On the Single Crystal X-Ray Diffraction Pattern of Calcite

Abstract

The method of analysis of double spectrometer rocking curves developed by L. P. Smith is reconsidered. Although from Smith's very general viewpoint, six experimental curves are needed for a complete analysis, it is shown that for rocking curves from calcite, taken with the usual type of double spectrometer, it should be possible to deduce the shape of the single crystal diffraction pattern from two rocking curves, the (1,+1) and (2,+2). A method of modifying the equations of the instrument to allow for a simple type of mosaic structure is indicated.The equations have been applied to rocking curves of Mo $K{\ensuremath{\alpha}}_{1}$ from calcite, supplied by L. G. Parratt. The method requires resolution of the observed curves into Fourier components, and a numerical method of doing this is described. The reliability of the components obtained can be tested by predicting the (1,-1) curve with them and comparing with experiment. In this way it is found that the curves are consistent as regards Fourier components of long period and large amplitude, but inconsistent in the short period, small amplitude components. A single crystal pattern is deduced, based mainly on the observed (1,-1) curve, with asymmetry as indicated by the (1,+1) and (2,+2) curves. It indicates that the crystals used do not have the flat-topped Darwin-Ewald-Prins diffraction pattern. Possible causes of the short period discrepancy have been investigated, but an adequate explanation has not been found.

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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
2
Average
Top 10%
Average
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