Synthetic Approaches to 2-Pyrrolidinone-5-carboxaldehyde

Jeffrey Deskus; Michael B. Smith; Tiberiu Simandan

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Synthetic Communications

Article . 1996 . Peer-reviewed

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https://dx.doi.org/10.1080/003...

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Synthetic Approaches to 2-Pyrrolidinone-5-carboxaldehyde

descriptionPublicationkeyboard_double_arrow_right Article 01 Aug 1996 English Publisher:Informa UK LimitedJournal:Synthetic Communications, volume 26, pages 3,137-3,150 (issn: 0039-7911, eissn: 1532-2432,

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Authors: Jeffrey Deskus; Michael B. Smith; Tiberiu Simandan;

doi: 10.1080/00397919608004620

Synthetic Approaches to 2-Pyrrolidinone-5-carboxaldehyde

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Abstract

Abstract We have examined routes for the preparation of 2-pyrrolidinone-5S-carboxaldehyde which include oxidation of 5-hydroxymethyl-2-pyrrolidinone and reduction of 5-oxoproline ethyl ester. Only the oxidation route proved satisfactory. Moffatt oxidation was most efficient but PCC oxidation gave modest yields of the desired aldehyde.

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University of Connecticut
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