Depsidone synthesis. IV. Caloploicin

descriptionPublicationkeyboard_double_arrow_right Article 01 Apr 1976 English Publisher:CSIRO PublishingJournal:Australian Journal of Chemistry, volume 29, pages 907-914 (issn: 0004-9425, eissn: 1445-0038,

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Authors: MV Sargent; P Vogel;

doi: 10.1071/ch9760907

Depsidone synthesis. IV. Caloploicin

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Abstract

The synthesis of the lichen depsidone caloploicin (2,4,7-trichloro-3-hydroxy-8-methoxy-1,6,9- trimethyldibenzo[b,e][l,4]dioxepin-11-one) (1) by oxidative coupling of 5'-chloro-2,2',4-trihydroxy-4- methoxy-3',6,6'-trimethylbenzophenone (23), and subsequent steps, is described.

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