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Review of Scientific Instruments
Article
License: CC BY
Data sources: UnpayWall
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Hal
Article . 2003
License: CC BY
Data sources: Hal
Review of Scientific Instruments
Article . 2003 . Peer-reviewed
Data sources: Crossref
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Porosity measurement by comparison of air volumes

Authors: Leclaire, Philippe; Umnova, Olga; Horoshenkov, Kirill; Maillet, Laurent;

Porosity measurement by comparison of air volumes

Abstract

A method for measuring the volume of a solid with arbitrary shape and the open porosity (volume fraction of the open pores) of air-saturated porous materials is proposed. The experimental principle is inspired from Beranek’s method [J. Acoust. Soc. Am. 13, 248 (1942)] based on the application of the ideal gas law to the gas surrounding the solid. The originality of the proposed method lies in the comparison of the volume of a measurement chamber containing the sample with that of an empty reference chamber. During a measurement, the reduction of volume in the measurement chamber due to the introduction of the solid is compensated by increasing the volume of a piston connected to the measurement chamber. An important aspect of this experimental system is that the influence of temperature can be considerably reduced as nearly the same variations of temperature apply simultaneously to the measurement and the reference chambers. A preliminary calibration experiment without sample in the measurement chamber is carried out in order to equalize the volumes of the two chambers. The calibration can be performed once and for all, thus minimizing the number of operations in the measurement process. The porosities of several materials are measured and compared to reference values. The precision and possible future improvements are discussed.

Related Organizations
Keywords

[SPI.MAT] Engineering Sciences [physics]/Materials, [PHYS.COND.CM-MS] Physics [physics]/Condensed Matter [cond-mat]/Materials Science [cond-mat.mtrl-sci]

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    popularity
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    Top 10%
    influence
    This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
47
Top 10%
Top 10%
Average
Green
hybrid