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A modular flow reactor for performing Curtius rearrangements as a continuous flow process

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 2008 English Publisher:Royal Society of Chemistry (RSC)Journal:Organic & Biomolecular Chemistry, volume 6, page 1,577 (issn: 1477-0520, eissn: 1477-0539, Copyright policy )
Authors: Jason P. Tierney; Ian R. Baxendale; Nikzad Nikbin; Christopher D. Smith; Steven V. Ley; Marcus Baumann;

doi: 10.1039/b801631n

pmid: 18421389

A modular flow reactor for performing Curtius rearrangements as a continuous flow process

Abstract

The use of a mesofluidic flow reactor is described for performing Curtius rearrangement reactions of carboxylic acids in the presence of diphenylphosphoryl azide and trapping of the intermediate isocyanates with various nucleophiles.

Related Organizations
Keywords

Azides, Molecular Structure, Carboxylic Acids, Urea, Stereoisomerism, Carbamates, Equipment Design, Sensitivity and Specificity, Chromatography, High Pressure Liquid, Mass Spectrometry

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    		 117
    popularity
    This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
    		 Top 10%
    influence
    This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
    		 Top 10%
    impulse
    This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
    		 Top 1%
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Found an issue? Give us feedback
citations
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
117
Top 10%
Top 10%
Top 1%
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