descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 2007 English Publisher:Royal Society of Chemistry (RSC)Journal:CrystEngComm, volume 9, page 879 (eissn: 1466-8033,

Authors: BRAGA D; GIAFFREDA SL; GREPIONI F; CHIEROTTI, Michele Remo; GOBETTO, Roberto; PALLADINO G; POLITO M.;

doi: 10.1039/b711983f

handle: 11585/51589 , 2318/25182

Solvent effect in a “solvent free” reaction

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Abstract

Vapour digestion of a mixture of solid [Fe(η5-C5H4–C5H4N)2] and solid pimelic acid HOOC(CH2)5COOH in the presence of solvent vapours generates co-crystals of different stoichiometry depending on the protic or aprotic nature of the solvent. The nature of the products has been ascertained by a combined use of SSNMR and X-ray diffraction.

Related Organizations

University of Turin
Italy
Alma Mater Studiorum University of Bologna
Italy

Keywords

CO-CRYSTAL FORMATION; SOLID-STATE; MECHANOCHEMICAL PREPARATION; ORGANOMETALLIC MATERIALS; COORDINATION NETWORK; ORGANIC-REACTIONS; ACID; COCRYSTAL; CAFFEINE; ISOMERS

1 Research products, page 1 of 1

CCDC 648403: Experimental Crystal Structure Determination
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