Synthesis of the parent resorcin[4]arene

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1999Publisher:Royal Society of Chemistry (RSC)Journal:Journal of the Chemical Society, Perkin Transactions 1 (issn: 0300-922X, eissn: 1364-5463,

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Authors: Hisatoshi Konishi; Hijiri Sakakibara; Kazuhiro Kobayashi; Osamu Morikawa;

doi: 10.1039/a905613k

Synthesis of the parent resorcin[4]arene

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Abstract

The treatment of 2,4-bis(allyloxy)benzyl alcohols with Sc(OTf)3 in acetonitrile produced a cyclic tetramer as the major product, which was deallylated by ammonium formate and PdCl2(PPh3)2 to produce the parent resorcin[4]arene.

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