Synthesis of Triethyl N-Formyl-N-phosphonomethylglycinate and Diethyl N-Formyl-N-phosphonomethylglycine and Studies of Their Rotational Conformers by Dynamic NMR

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1999 Australia Publisher:Royal Society of Chemistry (RSC)Journal:Journal of Chemical Research (issn: 0308-2342, eissn: 1364-5560,

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Authors: Ziora, Z; Cierpicki, T; Grembecka, J; Kafarski, P;

doi: 10.1039/a806474a

Synthesis of Triethyl N-Formyl-N-phosphonomethylglycinate and Diethyl N-Formyl-N-phosphonomethylglycine and Studies of Their Rotational Conformers by Dynamic NMR

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Abstract

Reaction of ethyl N-phosphonomethylglycinate with triethyl orthoformate gave a mixture of triethyl N-formyl-N-phosphonomthylglycinate (3) and diethyl N-formyl-N-phosphonomethylglycine (4), the rotational barriers of which have been investigated theoretically and experimentally.

Country

Australia

Related Organizations

University of Queensland
Australia
University of Queensland
Australia
Wrocław University of Science and Technology
Poland
Polish Academy of Sciences
Poland
Institute of Organic Chemistry
Poland

Keywords

N,n-Dimethylformamide, Acids, Bond, Barriers

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