Intermediates for Glucuronide Synthesis: 7-Hydroxycoumarin Glucuronide

Richard T. Brown; Feodor Scheinmann; Andrew V. Stachulski

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Journal of Chemical Research Synopses

Article . 1997 . Peer-reviewed

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https://dx.doi.org/10.1039/a70...

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Intermediates for Glucuronide Synthesis: 7-Hydroxycoumarin Glucuronide

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1997 English Publisher:Royal Society of Chemistry (RSC)Journal:Journal of Chemical Research (issn: 0308-2342, eissn: 1364-5560,

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Authors: Richard T. Brown; Feodor Scheinmann; Andrew V. Stachulski;

doi: 10.1039/a703397b

Intermediates for Glucuronide Synthesis: 7-Hydroxycoumarin Glucuronide

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Abstract

A convenient synthesis of the important metabolite 7-hydroxycoumarin glucuronide 3 is presented, including a first report of the β-imidate 11β, together with new preparations of the iodosugar 6 and α-imidate 11α: stability data on 11α and 11β are also given, and the importance of carefully controlled hydrolysis in the last step of the preparation of 3 is emphasised.

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