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Studies on the conditions of synthesis of picolinic acid by heterogeneous catalytic oxidation of 2-picoline

descriptionPublicationkeyboard_double_arrow_right Article 01 Sep 1998 English Publisher:Springer Science and Business Media LLCJournal:Catalysis Letters, volume 54, pages 149-152 (issn: 1011-372X, eissn: 1572-879X,

Authors: D. E. Babushkin; Galina A. Zenkovets; E. M. Al'kaeva; T. V. Andrushkevich;

doi: 10.1023/a:1019000610586

Studies on the conditions of synthesis of picolinic acid by heterogeneous catalytic oxidation of 2-picoline

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Abstract

Heterogeneous oxidation of 2-picoline over binary P–Ti, Sb–Ti, P–Sb, and V–Ti oxide catalysts was studied over the temperature range of 200–300°C. The vanadium–titanium catalysts based on titanium dioxide (anatase) were found to be the most selective for picolinic acid. With binary catalysts containing 20–50% of vanadium pentoxide, the selectivity for picolinic acid was 19–22% at the 36–74% conversion of 2-picoline. A distinguishing feature of these catalysts is regular surface stacking of V2O5 and TiO2 crystallites.

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