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Method for Assigning Structure of 1,2,3-Triazoles

descriptionPublicationkeyboard_double_arrow_right Article 29 Aug 2012 English Publisher:American Chemical Society (ACS)Journal:The Journal of Organic Chemistry, volume 77, pages 8,756-8,761 (issn: 0022-3263, eissn: 1520-6904, Copyright policy )
Authors: Frances Crowell; Andrew Anderson; Zachary Funk; Carl Brophy; Xavier Creary;

doi: 10.1021/jo301265t

pmid: 22894557

Method for Assigning Structure of 1,2,3-Triazoles

Abstract

1,4-Disubstituted-1H-1,2,3-triazoles 1 can easily be distinguished from the isomeric 1,5-disubstituted-1H-1,2,3-triazoles 2 by simple one-dimensional (13)C NMR spectroscopy using gated decoupling. The C(5) signal of 1 appears at δ ∼120 ppm, while the C(4) signal of 2 appears at δ ∼133 ppm. Computational studies also predict the upfield shift of C(5) of 1 relative to C(4) in 2.

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citations
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
138
Top 1%
Top 10%
Top 10%
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