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image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Powder Technologyarrow_drop_down
image/svg+xml Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao Closed Access logo, derived from PLoS Open Access logo. This version with transparent background. http://commons.wikimedia.org/wiki/File:Closed_Access_logo_transparent.svg Jakob Voss, based on art designer at PLoS, modified by Wikipedia users Nina and Beao
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Article . 2012 . Peer-reviewed
License: Elsevier TDM
Data sources: Crossref
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Master debinding curves for solvent extraction of binders in powder injection molding

Authors: Enneti, RK; Shivashankar, TS; Park, SJ; German, RM; Atre, SV;

Master debinding curves for solvent extraction of binders in powder injection molding

Abstract

Abstract This study successfully extends the master sintering curve concept to model removal of polymeric binders in powder injection molded bodies. In this demonstration the focus is solvent debinding. Master debinding curves (MDC) were used to estimate the activation energy for debinding. Binder removal curves were developed for solvent extraction of polyethylene glycol (PEG) from injection molded shapes made from silicon nitride doped with yttria and spinel (Si3N4 5% Y2O3 5% MgAl2O4). The extraction for different shapes incorporated a shape parameter in the standard master curve equation, giving activation energy of 12.4 kJ/mol extraction of PEG. Master debinding curves were also developed for wicking debinding. The analysis showed lower activation energies for solvent extraction and wicking compared to thermal debinding. The lower activation energy suggests easier removal by solvent or wicking versus pyrolysis. The study provides a unifying quantitative framework for comparing and predicting the effects of material, process and geometry on binder removal. The master debinding curves can be utilized in design and optimization of binder removal.

Country
Korea (Republic of)
Related Organizations
Keywords

SINTERING CURVE, Solvent debinding, NANOCRYSTALLINE, DECOMPOSITION CURVE, MOLDED PARTS, MODEL, CERAMICS, Activation energy, Wicking, Master debinding curves, KINETICS

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    influence
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Powered by OpenAIRE graph
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selected citations
These citations are derived from selected sources.
This is an alternative to the "Influence" indicator, which also reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Citations provided by BIP!
popularity
This indicator reflects the "current" impact/attention (the "hype") of an article in the research community at large, based on the underlying citation network.
BIP!Popularity provided by BIP!
influence
This indicator reflects the overall/total impact of an article in the research community at large, based on the underlying citation network (diachronically).
BIP!Influence provided by BIP!
impulse
This indicator reflects the initial momentum of an article directly after its publication, based on the underlying citation network.
BIP!Impulse provided by BIP!
38
Top 10%
Top 10%
Top 10%
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