Granular sludge is the key factor for an efficient operation of an upflow anaerobic sludge blanket (UASB) reactor. In order to monitor the granularity of anaerobic sludge, the determination of the granule size distribution is of vital importance. For this reason, several techniques have been proposed; however, they are either tedious, imprecise or expensive and hardly applicable in full-scale treatment plants. There was then the need for a simple and low-cost technique. This technique involves the determination of the settling velocities of a sludge sample and of extrapolating the corresponding diameters using a mathematical algorithm. In the proposed algorithm, the granules density was calculated, the flow regime was examined and finally the granule size distribution was obtained. Two very important correlations were suggested by the experimental results. The granule density and diameter were strongly correlated with the VSS/TSS ratio.